|
|
|
Scientific
background
|
LIF Labeling
agent
|
FAQ
|
|
|
Common fluorescent
tags for derivatization are listed in the table below :
|
For amine function (amines, amino acids, peptides, proteins…)
|
|
Primary and secondary amine
functions :
|
Fluorescein isothiocyante
(FITC)
|
488 nm
|
|
|
4-fluoro-7-nitrobenz-2-oxa-1,3-diazole
(NBD-F)
|
488 nm
|
|
|
Dansyl chloride 325 nm
|
325 nm
|
|
|
|
|
|
Primary amine function :
|
naphtalene 2,3- dicarboxaldehyde
(NDA)
|
442 nm
|
|
|
3-(4-carboxybenzoyl)-quinoline-2-carboxaldehyde
(CBQCA)
|
442 nm
|
|
|
fluorescamine
|
354 nm
|
|
|
orthophthaldialdehyde (OPA)
|
325 nm
|
|
|
|
|
|
For hydroxy function
|
|
alcohol
|
Fluorescein-5-carbonylazyde
|
488 nm
|
|
|
|
|
|
sugars
|
9-aminopyrene-1,4,6 trisulfonate
(APTS)
|
488 nm
|
|
|
9-aminonaphtalene-1,4,6
trisulfonate (ANTS)
|
354 nm
|
|
|
fluorescamine
|
354 nm
|
|
|
amino benzamide
|
325 nm
|
|
|
|
|
|
For thiol function (amino acids,
peptides, proteins…)
|
|
|
5-iodo-acetamido-fluorescein
(IAF)
|
488 nm
|
|
|
4-fluoro-7-nitrobenz-2-oxa-1,3-diazole
(NBD-F)
|
488 nm
|
|
For aldehyde and ketone functions
|
|
|
fluorescein-5-thiosemicarbazide
|
488 nm
|
|
For carboxylic function
|
|
|
5-bromomethyl fluorescein
|
488 nm
|
|
|
More about derivatization :
- Lunn G., Hellwig L.C. " Handbook
of derivatization reactions for HPLC " Wiley Interscience, New
York, 1998. (ISBN0-471-23888-0)
- Toshimasa Toyo'oka " Modern derivatization
methods for separation sciences " Wiley Interscience, New York,
1999. (ISBN0-471-98364-0)
- Bayle C., Couderc F. "Fluor-up
: Updated references on derivatization reactions for HPLC and
CE " , Picometrics Data Base, Picometrics, 2000.
|
 |
|